Research article

Conflicting behavior between powdering and flaking resistance under skin pass mill process in galvannealed interstitial free steel

  • Received: 14 May 2023 Revised: 24 July 2023 Accepted: 26 July 2023 Published: 09 August 2023
  • The failure of galvannealed (GA) coatings during press forming is an important issue for steel companies, because it results in a deteriorated product quality and reduced productivity. Powdering and flaking are thought to be the main failure modes in GA steel. However, these two modes currently lack a clear distinction, despite their different failure types. Therefore, in this study, we demonstrate that the different behaviors of these two failure modes are generated by the skin pass mill (SPM) condition and we discuss the underlying mechanism in detail using microstructural and simulation analyses. With the increase in steel elongation from 0% to 4.0% under milling force from 0 to 6 ton, a high compressive stress is produced up to −380 MPa on the surface of the steel sheet and the interface is correspondingly flattened from 0.96 to 0.53 μm in Ra. This flattening weakens the mechanical interlocking effect for adhesive bonding, deteriorating the flaking resistance from 41.1 to 65.2 hat-bead contrast index (hci). In addition, the GA coating layer becomes uniformly densified via the filling of pores under compressive stress in the layer. Furthermore, the ζ phase exhibits significant plastic deformation, leading to a uniform coverage of the coating surface; this helps to suppress crack propagation. Accordingly, the powdering resistance gradually improves from 4.2 to 3.5 mm. Consequently, with the increase in SPM-realized steel sheet elongation, the powdering resistance improves whilst the flaking resistance deteriorates. Significantly for the literature, this implies that the two failure modes occur via different mechanisms and it indicates the possibility of controlling the two coating failure modes via the SPM conditions.

    Citation: Hyungkwon Park, Young-Joong Jeong, Jin-Jong Lee, Chang-Hoon Lee, Bong Joo Goo, Yonghee Kim. Conflicting behavior between powdering and flaking resistance under skin pass mill process in galvannealed interstitial free steel[J]. AIMS Materials Science, 2023, 10(4): 637-651. doi: 10.3934/matersci.2023036

    Related Papers:

  • The failure of galvannealed (GA) coatings during press forming is an important issue for steel companies, because it results in a deteriorated product quality and reduced productivity. Powdering and flaking are thought to be the main failure modes in GA steel. However, these two modes currently lack a clear distinction, despite their different failure types. Therefore, in this study, we demonstrate that the different behaviors of these two failure modes are generated by the skin pass mill (SPM) condition and we discuss the underlying mechanism in detail using microstructural and simulation analyses. With the increase in steel elongation from 0% to 4.0% under milling force from 0 to 6 ton, a high compressive stress is produced up to −380 MPa on the surface of the steel sheet and the interface is correspondingly flattened from 0.96 to 0.53 μm in Ra. This flattening weakens the mechanical interlocking effect for adhesive bonding, deteriorating the flaking resistance from 41.1 to 65.2 hat-bead contrast index (hci). In addition, the GA coating layer becomes uniformly densified via the filling of pores under compressive stress in the layer. Furthermore, the ζ phase exhibits significant plastic deformation, leading to a uniform coverage of the coating surface; this helps to suppress crack propagation. Accordingly, the powdering resistance gradually improves from 4.2 to 3.5 mm. Consequently, with the increase in SPM-realized steel sheet elongation, the powdering resistance improves whilst the flaking resistance deteriorates. Significantly for the literature, this implies that the two failure modes occur via different mechanisms and it indicates the possibility of controlling the two coating failure modes via the SPM conditions.



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    [1] Shibli SMA, Meena BN, Remya R (2015) A review on recent approaches in the field of hot dip zinc galvanizing process. Surf Coat Tech 262: 210–215. https://doi.org/10.1016/J.SURFCOAT.2014.12.054 doi: 10.1016/j.surfcoat.2014.12.054
    [2] Marder AR (2000) The metallurgy of zinc-coated steel. Prog Mater Sci 45: 191–271. https://doi.org/10.1016/S0079-6425(98)00006-1 doi: 10.1016/S0079-6425(98)00006-1
    [3] Inui H, Okamoto NL, Yamaguchi S (2018) Crystal structures and mechanical properties of Fe-Zn intermetallic compounds formed in the coating layer of galvannealed steels. ISIJ Int 58: 1550–1561. https://doi.org/10.2355/isijinternational.ISIJINT-2018-066 doi: 10.2355/isijinternational.ISIJINT-2018-066
    [4] Yang D, Wang K, Zhou H, et al. (2023) Microstructure and properties of galvannealed coatings at different galvannealed time. Mater Lett 345: 134489. https://doi.org/10.1016/j.matlet.2023.134489 doi: 10.1016/j.matlet.2023.134489
    [5] Okamoto NL, Inomoto M, Adachi H, et al. (2014) Micropillar compression deformation of single crystals of the intermetallic compound ζ-FeZn13. Acta Mater 65: 229–239. https://doi.org/10.1016/j.actamat.2013.10.065 doi: 10.1016/j.actamat.2013.10.065
    [6] Garza LG, Van Tyne CJ (2007) Friction and formability of galvannealed interstitial free sheet steel. J Mater Process Tech 187: 164–168. https://doi.org/10.1016/j.jmatprotec.2006.11.062 doi: 10.1016/j.jmatprotec.2006.11.062
    [7] Kancharla H, Mandal GK, Kumar RR, et al. (2022) Effect of annealing time on coating microstructure, frictional and electrochemical behavior of galvannealed interstitial-free steel. J Mater Eng Perform 32: 5932–5945. https://doi.org/10.1007/s11665-022-07527-4 doi: 10.1007/s11665-022-07527-4
    [8] Arimura M, Urai M, Iwaya J, et al. (1995) Effects of press-forming factors and flash plating on coating exfoliation of galvannealed steel sheets. Galvatech'95, The Use and Manufacture of Zinc and Zinc Alloy Coated Sheet Steel Products Into the 21 st Century, 733–738.
    [9] Claus G, Dilewijns J, De Cooman B, et al. (1995) Determination of the process window for optimal galvannealing of Ti-IF steel. Proceedings' Galvatech 95'ISS, Chicago, 107–113.
    [10] Hong MH (2005) Correlation between the microstructure of galvannealed coatings and the defoliation during press forming. ISIJ Int 45: 896–902. https://doi.org/10.2355/isijinternational.45.896 doi: 10.2355/isijinternational.45.896
    [11] Lee KK, Lee IH, Lee CR, et al. (2007) In-situ observation in a scanning electron microscope on the exfoliation behavior of galvannealed Zn-Fe coating layers. Surf Coat Tech 201: 6261–6266. https://doi.org/10.1016/j.surfcoat.2006.11.021 doi: 10.1016/j.surfcoat.2006.11.021
    [12] Martin P, Handford MA, Packwood R, et al. (1992) Mechanical and structural study of Zn-Fe coatings on steel sheet. Galvatech'92, Amsterdam, 112–116.
    [13] Cheng C, Krishnardula V, Hahn H (2015) The effect of Al content in the coating on the flaking resistance of GA IF steels. International Conference on Zinc and Zinc Alloy Coated Steel Sheet, 96–103.
    [14] Han K, Lee I, Ohnuma I, et al. (2018) Micro-Vickers hardness of intermetallic compounds in the Zn-rich portion of Zn-Fe binary system. ISIJ Int 58: 1578–1583. https://doi.org/10.2355/isijinternational.ISIJINT-2018-111 doi: 10.2355/isijinternational.ISIJINT-2018-111
    [15] Park H, Jeong YJ, Lee K, et al. (2020) Effect of galvannealing temperature on coating microstructure evolution correlated to flaking degradation on galvannealed interstitial-free steel. Surf Coat Tech 404: 126446. https://doi.org/10.1016/j.surfcoat.2020.126446 doi: 10.1016/j.surfcoat.2020.126446
    [16] Park H, Jeong YJ, Lee K, et al. (2021) Correlation of interface microstructural features with the adhesive bonding strength of galvannealed interstitial-free steel. Met Mater Int 27: 3250–3259. https://doi.org/10.1007/s12540-020-00691-z doi: 10.1007/s12540-020-00691-z
    [17] Hamers AJ, Koesveld WV, Schoen JP (1998) Stone chipping resistance, press behaviour and coating roughness of galvannealed IF steels. Galvatech'98, Chiba, 597–602.
    [18] Park H, Jeong YJ, Lee K, et al. (2020) Interface exfoliation mechanism of galvannealed steel sheet in bead-slide during press-forming. Mater Today Commun 25: 101669. https://doi.org/10.1016/j.mtcomm.2020.101669 doi: 10.1016/j.mtcomm.2020.101669
    [19] Santos LA, Lopes LU, Wendhausen PAP (2014) Synthesis and characterization of the Fe-Zn intermetallic phases using the Rietveld Method. Rem-Rev Esc Minas 67: 181–184. http://dx.doi.org/10.1590/S0370-44672014000200008 doi: 10.1590/S0370-44672014000200008
    [20] Fluhrer J (2015) DEFORMTM 2D Version 8.1 User's Manual, Columbus, Ohio: Scientific Forming Technologies Corporation.
    [21] Quang P, Krishnaiah A, Hong SI, et al. (2009) Coupled analysis of heat transfer and deformation in equal channel angular pressing of Al and steel. Mater Trans 50: 40–43. https://doi.org/10.2320/matertrans.MD200823 doi: 10.2320/matertrans.MD200823
    [22] Wai Myint P, Hagihara S, Tanaka T, et al. (2017) Determination of the values of critical ductile fracture criteria to predict fracture initiation in punching processes. J Manuf Mater Process 1: 12. https://doi.org/10.3390/jmmp1020012 doi: 10.3390/jmmp1020012
    [23] Okamoto NL, Kashioka D, Inomoto M, et al. (2013) Compression deformability of Γ and ζ Fe-Zn intermetallics to mitigate detachment of brittle intermetallic coating of galvannealed steels. Scripta Mater 69: 307–310. https://doi.org/10.1016/j.scriptamat.2013.05.003 doi: 10.1016/j.scriptamat.2013.05.003
    [24] Nikitin I, Besel M (2008) Residual stress relaxation of deep-rolled austenitic steel. Scripta Mater 58: 239–242. https://doi.org/10.1016/j.scriptamat.2007.09.045 doi: 10.1016/j.scriptamat.2007.09.045
    [25] Bhujangrao T, Veiga F, Penalva M, et al. (2022) Three-dimensional finite element modelling of sheet metal forming for the manufacture of pipe components: symmetry considerations. Symmetry 14: 228. https://doi.org/10.3390/sym14020228 doi: 10.3390/sym14020228
    [26] Wang W, Hua D, Zhou Q, et al. (2023) Effect of a water film on the material removal behavior of Invar during chemical mechanical polishing. Appl Surf Sci 616: 156490. https://doi.org/10.1016/j.apsusc.2023.156490 doi: 10.1016/j.apsusc.2023.156490
    [27] Alpas AT, Inagaki J (2000) Effect of microstructure on fracture mechanisms in galvannealed coatings. ISIJ Int 40: 172–181. https://doi.org/10.2355/isijinternational.40.172 doi: 10.2355/isijinternational.40.172
    [28] Nunomura Y, Takasugi T (2003) Plastic deformation and fracture behavior of galvannealed coating. ISIJ Int 43: 454–460. https://doi.org/10.2355/isijinternational.43.454 doi: 10.2355/isijinternational.43.454
    [29] Ploypech S, Boonyongmaneerat Y, Jearanaisilawong P (2012) Crack initiation and propagation of galvanized coatings hot-dipped at 450 ℃ under bending loads. Surf Coat Tech 206: 3758–3763. http://dx.doi.org/10.1016/j.surfcoat.2012.03.029 doi: 10.1016/j.surfcoat.2012.03.029
    [30] Ochiai S, Okuda H, Iwamoto S, et al. (2005) Multiple-cracking phenomenon of the galvannealed coating layer on steels under thermal and tensile stresses. Metall Mater Trans A 36: 1807–1816. https://doi.org/10.1007/s11661-005-0044-0 doi: 10.1007/s11661-005-0044-0
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